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| Luyten, S.; Smeyers-Verbeke, J.; Massart, D.L.. |
| In clinical chemistry it can be very useful to have a rapid method for the determination of trace elements in biological material available. Because the classical wet digestion method which is generally used for the destruction of biological materials requires much attention, two procedures were tried which should be less time consuming or require less attention. The two new procedures which are the soluene (a quaternary ammonium hydroxide) method of Jackson (1) and the method of Adrian (2) utilizing pressure were applied to the determination of Cu and Zn in human brain tissue and in fish meal by atomic absorption spectroscopy. |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Chemical analysis; Trace metals. |
| Ano: 1973 |
URL: http://www.vliz.be/nl/open-marien-archief?module=ref&refid=3474 |
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| Mertens, J.; Massart, D.L.. |
| A simple and rapid method for the determination of nitrate in seawater of high nitrate content (>1 ppm) is proposed. The absorption of the nitrate ion is measured at 210 and 220 mµ. The sample is treated with a measured quantity of hydrochloric acid to eliminate the carbonate and bicarbonate interferences and measured against a nitrate free blank prepared by reduction of the nitrate to ammonia with Raney nickel. The addition of HCl permits also storage of the sample without special precautions and the use of the blank eliminates the most serious of the interferences (bromide) expected in seawater. The interference of organic matter limits however the applicability of the method to concentrations higher than 1 ppm. |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Marine environment; Nitrates; Spectroscopy. |
| Ano: 1971 |
URL: http://www.vliz.be/nl/open-marien-archief?module=ref&refid=3424 |
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